ATD Tools 5928 Guía de usuario Pagina 10
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Contents
vi
Ambient Pressure Calibration .................................... 259
Checking the Pneumatics for the
TurboMatrix Series PPC Units...................................260
Tube and Trap Impedance Calibration for
the TurboMatrix 650 ATD ......................................... 262
Removing and Replacing the Cold Trap....................269
Removing the Cold Trap .....................................270
Replacing the Cold Trap...................................... 275
Cold Trap Maintenance..............................................277
Conditioning the Trap.......................................... 277
De-Icing the Cold Trap........................................278
Repacking the Cold Trap.....................................279
Changing the Trap Filter Disks............................281
Packing Sample Tubes ............................................... 284
Stainless Steel Tubes ........................................... 285
Glass and Glass-Lined Stainless Steel Tubes......285
Gauze-Loading Accessory...................................286
Conditioning Packed Sample Tubes.................... 287
Storage and Lifetime of Packed Tubes................ 290
Cleaning the ATD Sample Tray.................................291
Changing the Fuse......................................................291
Theory of Thermal Desorption ...................295
Introduction ................................................................297
Manual Pneumatics..............................................297
Programmable Pneumatic Control (PPC)............ 297
Modes of Operation............................................. 299
Trap Clean Mode........................................................ 301
Tube Conditioning......................................................301
Two-Stage Desorption - Sample Analysis .................303
Overlapping Tube Desorption ............................. 306
Automated Leak Testing ............................................307
Pressurization of the Tube for Leak Testing........307
Primary and Secondary Leak Test of the
Sample Tube ........................................................ 308
Leak Testing the Cold Trap.................................309
Number of Leak Test Retries............................... 309
Carrier Gas Purge of the Sample Tube.......................310
Cold Trap Flow Configuration...................................313
Single-Stage versus Two-Stage Desorption...............314
Single Stage (Non-PerkinElmer)......................... 314
Two Stage Desorption (PerkinElmer ATD) ........315
Practical Applications of Thermal Desorption...........316
- TURBOMATRIX SERIES 1
- THERMAL DESORBERS 1
- TurboMatrix Series 3
- Thermal Desorbers 3
- User’s Guide 3
- M041-3331 E January 2007 4
- Contents 10
- Introduction 1 19
- Introduction 21
- About this Manual 24
- Unpacking the Instrument 25
- Safety Information 28
- Electrical Safety 29
- Mechanical Hazard 32
- Chemicals 32
- Handling Compressed Gases 33
- Extreme Temperatures 35
- Waste Disposal 36
- Sample Tubes 36
- Products 37
- Installation and Setup 2 39
- Pre-installation Checklist 41
- Installation and Setup 42
- Laboratory Requirements 43
- Electrical Connections 47
- Electrical Surge 48
- Chromatograph 49
- The ATD/TD Input/Output Port 51
- TD Output Signals 51
- TurboMatrix I/O Port 53
- ATD/TD Input Signals 54
- Timed Event Relays 55
- Connecting the ATD/TD to the 55
- TURBOMATRIX 56
- HP 5890 and HP 6890 57
- Transfer Line 63
- Access Hole 63
- Installation at the ATD/TD 65
- Panel of the GC 69
- Bad Cuts 71
- Good Cut 71
- Connecting a Packed Column 74
- Column to the TD 76
- Gas Supply Specifications 78
- Gas Connections 79
- Carrier In 83
- Supply Pressure 83
- 90 psi/620 kPa 83
- Standard In 83
- Dry Air In 83
- Connecting the Dryer Assembly 84
- Setting the Carrier Gas Flows 85
- Series 100 TD and 150 ATD 86
- Operation 3 91
- Attention: 96
- Operation 100
- 100 TD and 150 ATD 101
- Creating a Sequence 102
- Editing a Sequence 104
- Status Tab 104
- Temperature Tab 105
- Timing Tab 107
- The Options Tab 111
- Operating Modes 115
- Pneumatics Tab 117
- The Log Tab 118
- Method Editor 120
- Preferences 123
- Calculator 123
- Maintenance Tab 124
- Preferences Tab 125
- Config Tab 127
- Setup Tab 128
- Connect Tab 132
- Loading Tubes 133
- Shutdown 139
- Status Line 140
- The Run Tab 141
- Loading the ATD Carousel 181
- Accessories 4 189
- <> 190
- Options Board 191
- Accessories 192
- BCD Interface 193
- Tubes and Caps 194
- Internal Standard Accessory 199
- Principle of Operation 201
- Operation of the IS Accessory 201
- Setting the IS Flow Rates 203
- TD Control Software 207
- Online Sampling Accessory 208
- AutoSystem XL or 209
- Clarus 500 GC 209
- Method Development 5 211
- Method Development 213
- Analytical Objectives 213
- Setting System Parameters 216
- High Temperature Operation 223
- Carrier Gas Flow Rates 224
- Phase Sampling 226
- *Pyridine 116 78 233
- Aniline 184 2200 233
- Setting Sample Split Ratios 236
- Single Split Operation 238
- SplitOutlet 2 239
- Double-Split Operation 240
- Vaporizing a Liquid Standard 244
- Sample Tube 245
- Atmosphere 246
- Sample Integrity Testing 247
- Sample Archiving 247
- Routine Maintenance 6 249
- Routine Maintenance 251
- Cleaning the Instrument 252
- Cleaning and Decontamination 252
- Carrier Gas 253
- Adsorbent Storage 253
- Sample Tubes and Storage Caps 254
- Spectrometer 254
- Covers of the ATD 255
- Loosen Screw 256
- (Do not remove the screw) 256
- Remove Screw 256
- Door Latch 256
- Mobile Seals 257
- TD Mobile Seal 260
- ATD Mobile Seal 261
- Leak Testing 263
- Standard Leak Test 265
- Impedance Calibration 265
- Column Leak Test 265
- GC Temp Calib 266
- Ambient Pressure Calibration 267
- TurboMatrix Series PPC Units 268
- Figure 73 Filter in Place 271
- Removing the Cold Trap 278
- Replacing the Cold Trap 283
- Cold Trap Maintenance 285
- De-Icing the Cold Trap 286
- Repacking the Cold Trap 287
- DesorbAdsorb 288
- Packing Sample Tubes 292
- Stainless Steel Tubes 293
- Gauze-Loading Accessory 294
- Changing the Fuse 299
- Cleaning the ATD Sample Tray 299
- Figure 84 Replacing the Fuse 301
- Theory of Thermal Desorption 306
- Modes of Operation 307
- Trap Clean Mode 309
- Tube Conditioning 309
- Analysis 311
- Overlapping Tube Desorption 314
- Automated Leak Testing 315
- Leak Testing the Cold Trap 317
- Number of Leak Test Retries 317
- Cold Trap Flow Configuration 321
- Desorption 322
- Techniques 325
- Sampling Techniques 8 327
- Sampling Techniques 330
- (min) timesamplingx U 331
- )(mg/m conc 331
- Zx 24.45 332
- Analyte Mass 337
- Molecular 338
- Component 338
- Atmospheric 339
- Concentration 339
- 1/3 of the limit 341
- Purge and Trap 342
- Soil Probes 342
- Sampling Resins and Ointments 345
- Sampling Solids 346
- Troubleshooting 9 349
- Troubleshooting 351
- Status Messages 351
- Instrument Fault Conditions 360
- Fatal Errors 372
- Edition, (Glasgow, 1996), p27 373
- The Cold Trap Does Not Cool 375
- Sample Carryover 376
- System Contamination 378
- Wide Boiling Range 384
- Appendices 10 387
- Appendix A Customer Service 389
- Limitations 390
- Appendix C References 391
- Appendices 392
- Helium Flow Rates 396
- Hydrogen Flow Rates 398
- Nitrogen Flow Rates 400
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